AODOP                                                Distillation – Operating Problems

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Performance Objectives:
  Pass Fail
Topic 1: Feed Problems
     
1.1 Explain the role of feed rate in maintaining column equilibrium. ____   ____
     
1.2 Identify problems that can occur when the feed rate is incorrect. ____   ____
     
1.3 Describe conditions that can lead to three operating problems: overloading, flooding, and puking. ____   ____
     
1.4 Describe some mechanical causes of overloading. ____   ____
     
1.5 Explain how to identify a flooded condition in a distillation tower. ____   ____
     
1.6 Explain how a liquid flood can be broken. ____   ____
     
1.7 Explain how flooding can be prevented or controlled. ____   ____
     
1.8 Identify process disturbances that can result from changes in the feed to a distillation tower. ____   ____
     
1.9 Identify problems that can show up during the startup of a distillation system. ____   ____
     
     
Topic 2: Reflux Problems    
     
2.1 Explain what reflux is. ____   ____
     
2.2 Describe what can happen if the amount of reflux going back to the column is not correct. ____   ____
     
2.3 Identify typical disturbances that can occur in shell and tube condensers and fin-fan condensers. ____   ____
     
     
Topic 3: Reboiler Problems    
     
3.1 Describe sources of heat input for a distillation tower at your site. ____   ____
     
3.2 Explain the role of reboiler operation in maintaining column equilibrium. ____   ____
     
3.3 Identify problems that can occur when the reboiler is operated incorrectly. ____    ____
     
3.4 Identify typical disturbances that can occur in shell and tube reboilers and fired reboilers. ____   ____
     
3.5 Define over-fractionation. ____    ____


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Performance Evaluator’s Name (Print):____________________________

Date Completed:____________________________